JPS6118540B2 - - Google Patents

Info

Publication number

JPS6118540B2

JPS6118540B2 JP8067880A JP8067880A JPS6118540B2 JP S6118540 B2 JPS6118540 B2 JP S6118540B2 JP 8067880 A JP8067880 A JP 8067880A JP 8067880 A JP8067880 A JP 8067880A JP S6118540 B2 JPS6118540 B2 JP S6118540B2

Authority

JP

Japan

Prior art keywords

trans

liquid crystal

cyclohexanecarboxylic acid

ester

compound

Prior art date

1980-06-14

Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

Expired

Links

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• 239000004973 liquid crystal related substance Substances 0.000 claims description 16
• 239000000203 mixture Substances 0.000 claims description 10
• 150000002148 esters Chemical class 0.000 claims description 6
• 125000000217 alkyl group Chemical group 0.000 claims description 3
• 229910052799 carbon Inorganic materials 0.000 claims description 3
• 125000004432 carbon atom Chemical group C* 0.000 claims description 3
• 125000000113 cyclohexyl group Chemical group [H]C1([H])C([H])([H])C([H])([H])C([H])(*)C([H])([H])C1([H])[H] 0.000 claims 2
• 150000001875 compounds Chemical class 0.000 description 15
• YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 9
• -1 trans-4-(trans-4'-substituted cyclohexyl)-cyclohexanecarboxylic acid Chemical class 0.000 description 7
• FYSNRJHAOHDILO-UHFFFAOYSA-N thionyl chloride Chemical compound ClS(Cl)=O FYSNRJHAOHDILO-UHFFFAOYSA-N 0.000 description 6
• JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 4
• 239000000463 material Substances 0.000 description 4
• 230000000704 physical effect Effects 0.000 description 4
• JXPGQFKJNKWDKP-UHFFFAOYSA-N 4-(4-propylcyclohexyl)cyclohexane-1-carboxylic acid Chemical compound C1CC(CCC)CCC1C1CCC(C(O)=O)CC1 JXPGQFKJNKWDKP-UHFFFAOYSA-N 0.000 description 3
• HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
• 239000013078 crystal Substances 0.000 description 3
• NGNBDVOYPDDBFK-UHFFFAOYSA-N 2-[2,4-di(pentan-2-yl)phenoxy]acetyl chloride Chemical compound CCCC(C)C1=CC=C(OCC(Cl)=O)C(C(C)CCC)=C1 NGNBDVOYPDDBFK-UHFFFAOYSA-N 0.000 description 2
• SJTBRFHBXDZMPS-UHFFFAOYSA-N 3-fluorophenol Chemical compound OC1=CC=CC(F)=C1 SJTBRFHBXDZMPS-UHFFFAOYSA-N 0.000 description 2
• LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
• 238000000921 elemental analysis Methods 0.000 description 2
• 238000004519 manufacturing process Methods 0.000 description 2
• 238000000034 method Methods 0.000 description 2
• UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 description 2
• HORNXRXVQWOLPJ-UHFFFAOYSA-N 3-chlorophenol Chemical compound OC1=CC=CC(Cl)=C1 HORNXRXVQWOLPJ-UHFFFAOYSA-N 0.000 description 1
• MTNZGYZWCQZBFV-UHFFFAOYSA-N 4-(4-propylcyclohexyl)cyclohexane-1-carbonyl chloride Chemical compound C1CC(CCC)CCC1C1CCC(C(Cl)=O)CC1 MTNZGYZWCQZBFV-UHFFFAOYSA-N 0.000 description 1
• BKZWTOBKQBHRIN-UHFFFAOYSA-N C(CC)C1C(CCCC1)(C(=O)O)C1CCCCC1 Chemical compound C(CC)C1C(CCCC1)(C(=O)O)C1CCCCC1 BKZWTOBKQBHRIN-UHFFFAOYSA-N 0.000 description 1
• PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 1
• 239000008186 active pharmaceutical agent Substances 0.000 description 1
• 238000001035 drying Methods 0.000 description 1
• 238000010438 heat treatment Methods 0.000 description 1
• 230000007935 neutral effect Effects 0.000 description 1
• 230000003287 optical effect Effects 0.000 description 1
• 239000000126 substance Substances 0.000 description 1
• 230000007704 transition Effects 0.000 description 1
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1